Submitting
Samples / Quantities Needed General guidelines for submitting
Samples. BETA does not need information which you feel may
breach the confidentiality of your product. Analysis can be done on almost
any solid, liquid, or gas containing carbon Products may be submitted in
their retail containers, or in sub-sample containers. - Solid materials
may be placed in zip-lock bags.
- Liquids may be placed in plastic or glass
vials
- Gases may be sealed in Pyrex or quartz 9.5 mm diameter tubes.
(contact the lab prior to submitting gases) Useful information you
can provide for each sample (but not required) is as follows. - Approximate
carbon content (weight of carbon to total weight of the sample),
Water content - Flammability
- Presence or absence of volatile compounds (e.g. alcohol)
- Presence
or absence of non-combustible organic compounds (e.g. graphite)
CATEGORY
1 vs. CATEGORY 2 material status - CATEGORY 1 materials consist of relatively
high carbon contents, low flammability, and low volume. They are generally everything
but highly flammable materials, explosive materials and materials with more than
15% carbon. They are charged at a lower rate.
- CATEGORY 2 samples are
generally flammables such as gasoline and fuel additives, and products with less
than 15% carbon contents such as detergents, shampoos, and body washes. Highly
acidic or highly alkaline products and highly heterogenous products would also
be CATEGORY 2 materials. These are charged at a higher rate.
One
sample-datasheet needs to be submitted with each sample. - These are
available to fill out either on-line, or to download as a PDF.
An
MSDS must be sent when available. - If an MSDS is not available, it
is the manufacturers responsibility to inform BETA of any health or environmental
concerns which BETA staff may be exposed to in handling of the product.
The
carbon content of the product must be high enough to be able to extract and measure.
- BETA has analyzed detergents with carbon contents as low as 0.07
%, so this can be very low.
Contact BETA for discussion prior to
submitting materials which may require special facilities for the handling of
toxic or hazardous substances. Submitting a sample that is truly representative
of the manufactured product is essential for an accurate result. - It
is important to mix well prior to sub-sampling for carbon-14 analysis. ASTM method
D7026-04 discusses sampling requirements associated with submitting samples for
biobased content analysis. The Standard Guide can be downloaded from the ASTM
website (www.astm.org).
Recommended Quantities The quantity
of product required depends upon the carbon content and flammability of the product.
The quantities listed in the table below are general recommendations.
| Fluids | | | |
| Non-combustible Fluids | | 20-30
mls | (0.7+ fl oz) | | Examples | Oils | | |
| | Detergents & cleansers | | |
| | Inks/dyes/pigments | | |
| | Lubricants | | |
| | Waxes | | |
| Combustible Fluids/Fuels | | 1-5 ml | (0.04+
fl oz) | | Examples | biodiesel | | |
| | gasoline | | |
| | ethanol | | | | | solvents | | |
| Solids | | 10-20
grams | (0.35+ oz) | | Examples | Plastics/polymers/films | | |
| | Paper/paper products | | |
| | construction materials/composites | | |
| | Textiles | | | |